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Extensive analysis of your TEM photos (G) away from graphite needles inside samples increasing immediately after 8 minute on the 2nd broadening techniques in the step 1,600 W demonstrably shows the new phase conversion process process from graphite so you can diamond. The brand new white boxes would be the section to the related expanded photographs and FFT photos lower than, as well as the purple and you may light arrows suggest the brand new flat length. (H) and you can (H-1) would be the HADDF and you can bright occupation TEM images for the next graphite needle, respectively, to your involved enlarged photos and you will FFT images less than. The new EELS spectra (I) of one’s additional sites marked because of the red points from some other phase transforming needle revealed in the (H)/(H-1).
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(J)/(J-1) Outline of one’s stage conversion process of graphite so you can diamond in the graphite needle mature to the cauliflower-for example particles. Understand so it incredible periodicity changing techniques, HRTEM specifications for the freshly molded coating was performed (Fig. 2). The fresh 0-s sample (Fig. 2A) displays highest pole-including diamond deposits evidenced because of the diffraction locations on the diamond (111) direction from the inset Fourier alter (FFT) picture.
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